Pengaruh Temperatur Dan Waktu Pengovenan Tulang Sapi Timor Terhadap Hasil Uji FTIR

  • Makxy Melian Melian(1)
    teknik mesin
  • Dominggus G. H. Adoe(2*)
    Universitas Nusa Cendana
  • Erich U. K. Maliwemu(3)
    Universitas Nusa Cendana
  • (*) Corresponding Author

Abstract

This study evaluates the effect of temperature and oven time on the results of the Fourier Transform Infrared Spectroscopy (FTIR) test on Timorese cow bones. Beef bones from East Nusa Tenggara, which are rich in calcium and phosphorus, are processed through cleaning, boiling, and soaking H2O2 before calcining at various temperatures (100°C, 200°C, 300°C) and duration (1 and 2 hours). The FTIR results showed significant changes in the chemical structure of the bones, with variations in temperature and baking time affecting the quality and characteristics of the bones. The study concluded that the precise setting of the ovening parameters can improve the quality of beef bone-based products, such as hydroxyapatite.

 

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References

Anon. 1998. “P . A . H I L L , B .D .S ., F .D .S ., M .O R T H ., B .S C , M .S C ., P H .D .” 25:101–7.

Arsista, Dede, Yosi Kusuma, Eriwati Departemen, Ilmu Material, and Kedokteran Gigi. 2021. “Penggunaan Atr-Ftir (Attenuated Total Reflection-Fourier Transform Infrared Spectroscopy) Pada Kedokteran Gigi.” Jurnal Material Kedokteran Gigi 1–10. doi: 10.32793/jmkg.v10i2.904.

Badan Pusat Statistik. 2021. “Provinsi Nusa Tenggara Timur Dalam Jumlah.”

Barakat, Nasser A. M., Myung Seob Khil, A. M. Omran, Faheem A. Sheikh, and Hak Yong Kim. 2009. “Extraction of Pure Natural Hydroxyapatite from the Bovine Bones Bio Waste by Three Different Methods.” Journal of Materials Processing Technology 209(7):3408–15. doi: 10.1016/j.jmatprotec.2008.07.040.

Costantino, P. D., and C. D. Friedman. 1994. “Synthetic Bone Graft Substitutes.” Otolaryngologic Clinics of North America 27(5):1037–74. doi: 10.1046/j.1440-1622.2001.2128.x.

Haley, Jennifer Anne. 2001. “Information To Users Umi.” Dissertation 274.

Hardiyanti. 2016. “Uin Alauddin Makassar.” Uin Alauddin Makasar 1–86.

Herdiana. 2013. “Pengaruh Asam, Basa, Metode Ektraksi Dan Metode Pengeringan Terhadap Viskositas Gelatin.” Journal of Chemical Information and Modeling 53(9):1689–99.

Hutajulu, Adven. 2017. “Sintesis Dan Karakterisasi Material Biokomposit Polylactic Acid (PLA) Berpenguat Serbuk Tulang Sapi Sebagai Kandidat Bahan Tulang Buatan.” Institut Teknologi Sepuluh Nopember, Surabaya 1–124.

Istifarah, Aminatun, and Prihartini Widiyanti. 2012. “Sintesis Dan Karakterisasi Komposit Hidroksiapatit Dari Tulang Sotong (Sepia Sp.)-Kitosan Untuk Kandidat Bone Filler.” Skripsi Fakultas Matematika Dan Ilmu Pengetahuan Alam 1–55.

Jaggi, Neena, and D. R. Vij. 2006. “Chapter 9 Fourier Transform Infrared.” Handbook of Applied Solid State Spectroscopy 411–50.

Jonathan Adrianto, Anderesas Pandu Setiawan. 2019. “Eksperimen Dengan Media Tulang Sapi Sebagai Media Alternatif Produk Interior.” Jurnal Intra 7(2):292–97.

Kartikasari, Niva Dian. 2014. “Sintesis Dan Karakterisasi Hidroksiapatit Dari Cangkang Keong Sawah (Pila Ampullaceal) Dengan Porogen Lilin Sarang Lebah Sebagai Aplikasi Scaffold.”

Kusrini, Eny, and Muhammad Sontang. 2012. “Characterization of X-Ray Diffraction and Electron Spin Resonance: Effects of Sintering Time and Temperature on Bovine Hydroxyapatite.” Radiation Physics and Chemistry 81(2):118–25. doi: 10.1016/j.radphyschem.2011.10.006.

Marwanto, Melisa Oktaviani Silitinga, Yudhi Harini Bertham, Merakati Handajaningsih, and Prasetyo. 2023. “Azolla Compost-Based Organomineral Fertilizer for Increasing N Uptake, Growth, and Yield of Green Onion.” AIP Conference Proceedings 2583(3):189–96. doi: 10.1063/5.0116207.

Mohd Pu’ad, N. A. S., P. Koshy, H. Z. Abdullah, M. I. Idris, and T. C. Lee. 2019. “Syntheses of Hydroxyapatite from Natural Sources.” Heliyon 5(5):e01588. doi: 10.1016/j.heliyon.2019.e01588.

Ooi, C. Y., M. Hamdi, and S. Ramesh. 2007. “Properties of Hydroxyapatite Produced by Annealing of Bovine Bone.” Ceramics International 33(7):1171–77. doi: 10.1016/j.ceramint.2006.04.001.

Oyerinde, A., and E. Bello. 2016. “Use of Fourier Transformation Infrared (FTIR) Spectroscopy for Analysis of Functional Groups in Peanut Oil Biodiesel and Its Blends.” British Journal of Applied Science & Technology 13(3):1–14. doi: 10.9734/bjast/2016/22178.

Perwitasari, Dyah Suci. 2008. “Hidrolisis Tulang Sapi Menggunakan HCl Untuk Pembuatan Gelatin.” Makalah Seminar Nasional Soebardjo Brotohardjono “Pengolahan Sumber Daya Alam Dan Energi Terbarukan” 1–9.

Prabaningtyas, R. Aj. Mahardhika Safanti. 2017. “Karakterisasi Hidroksiapatit Dari Kalsit (PT. Dwi Selo Giri Mas Sidoarjo) Sebagai Bon Graft Sintesis Menggunakan X-Ray Diffraction (XRD) Dan Fourier Transform Infra Red (FTIR).” Digital Repostpry Universitas Jember 3(3):96–104.

Rocha, J. H. G., A. F. Lemos, S. Agathopoulos, P. Valério, S. Kannan, F. N. Oktar, and J. M. F. Ferreira. 2005. “Scaffolds for Bone Restoration from Cuttlefish.” Bone 37(6):850–57. doi: 10.1016/j.bone.2005.06.018.

Sandyawan, Ignasius, Tolu Lele, Erich U. K. Maliwemu, and Dominggus G. H. Adoe. 2022. “Karakterisasi Biomaterial Hidroksiapatit Dari Cangkang Kerang Ale-Ale Pantai Oesapa Kota Kupang.” Seminar Nasional Kimia Dan Pendidikan Kimia I, Universitas Nusa Cendana 56–62.

Silverstein, Robert M., Francis X. Webster, David J. Kiemle, and David L. Bryce. n.d. “Eighth Edition Spectrometric Identification of Organic Compounds Mass Spectrometry 1.”

Sugiharto, Endang Widiastuti, and Hanny Indrat Wahyuni. 2021. Buku Ajar Fisiologi Ternak.

Suhu, Pengaruh, Dan Waktu, Kalsinasi Terhadap, Kemurnian Hidroksiapatit, Berbasis Tulang, Sapi Dengan, Metode Presipitasi, Yoppy Pratama, and Jurusan Teknik Mesin. 2023. Mochamad Arif Irfa’i.

Szcześ, Aleksandra, Lucyna Hołysz, and Emil Chibowski. 2017. “Synthesis of Hydroxyapatite for Biomedical Applications.” Advances in Colloid and Interface Science 249:321–30. doi: 10.1016/j.cis.2017.04.007.

Weiss, P., M. Lapkowski, R. Z. Legeros, J. M. Bouler, A. Jean, and G. Daculsi. 1997. “FTIR Spectroscopic Study of an Organic / Mineral Composite for Bone and Dental Substitute Materials .” Materials Science 8(10):621–29.

YessyWarastuti, Emil Budianto, and Darmawan. 2015. “Jurnal Sains Materi Indonesia SINTESIS DAN KARAKTERISASI MEMBRAN KOMPOSIT HIDROKSIAPATIT TULANG SAPI-KHITOSAN-POLI ( VINIL Bahan Dan Alat.” Sains Materi Indonesia 16(3000):83–90.

Yuliana, Reflin, Erwin Abdul Rahim, Jaya Hardi, Jl Soekarno, Hatta Km, Kampus Bumi Tadulako, and Tondo Palu. 2017. “SINTESIS HIDROKSIAPATIT DARI TULANG SAPI DENGAN METODE BASAH PADA BERBAGAI WAKTU PENGADUKAN DAN SUHU SINTERING [Synthesis of Hydroxyapatite from Cow Bones Under Wet Method at Various of Stirring Times and Sintering Temperatures].” KOVALEN 3(3):201–10.

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Published
2024-10-31
How to Cite
Melian, M., Adoe, D., & Maliwemu, E. (2024). Pengaruh Temperatur Dan Waktu Pengovenan Tulang Sapi Timor Terhadap Hasil Uji FTIR. LONTAR Jurnal Teknik Mesin Undana, 11(02), 8-13. https://doi.org/10.35508/ljtmu.v11i02.18028

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