PERBANDINGAN KARAKTERISTIK PIM BERBASIS POLIVINIL KLORIDA, DI-(2- ETHYLHEXYL) PHOSPHORIC ACID DAN ASAM OLEAT SEBELUM DAN SESUDAH EKSTRAKSI Zn(II) DALAM SUASANA ASAM
-
Fidelis Nitti(1*)
Program Studi Kimia, Fakultas Sains dan Teknik, Universitas Nusa Cendana
-
Suwari .(2)
Program Studi Kimia, Fakultas Sains dan Teknik, Universitas Nusa Cendana
-
Yoana Fransiska De Chantal Kedang(3)
Program Studi Kimia, Fakultas Sains dan Teknik, Universitas Nusa Cendana
(*) Corresponding Author
Keywords:
PIM, Ekstraksi Zn(II)
Abstract
Telah dilakukan penelitian dengan judul Perbandingan Karakteristik PIM Berbasis Polivinil Klorida,
Di-(2-Ethylhexyl) Phosphoric Acid dan Asam Oleat Sebelum dan Sesudah Ekstraksi Zn(II) dalam
Suasana Asam. Penelitian ini bertujuan untuk mengetahui kemampuan PIM dalam mengekstraksi
Zn(II) serta perbandingan karakteristik sifat fisik dan kimia pada PIM sebelum dan sesudah
dilakukan ekstraksi Zn(II) dalam suasana asam. Hal ini ditentukan dengan mengaplikasikan PIM
untuk ekstraksi Zn(II) yang kemudian diuji sifat fisika dan kimianya berupa pengukuran Water
Contact Angle, Water Uptake, Tensile Strength dan % Elongation serta karakterisasi PIM
menggunakan Fourier Transform Infrared Spectroscopy (FTIR) dan Scanning Electron Microscope (SEM) untuk mengetahui kinerja dan stabilitas PIM dalam aplikasi selanjutnya. Hasil penelitian menunjukkan bahwa PIM mampu mengekstraksi Zn(II) dalam suasana asam sebanyak 21,24 mg/L dari konsentrasi 24 mg/L atau efisiensi pemisahan sebesar 88,5%. Sedangkan perbandingan karakterisasi FTIR , SEM serta nilai pengujian sifat fisik dan kimia sebelum dan sesudah ekstraksi tidak menunjukan perbedaan yang signifikan dimana membran masih bersifat hidrofilik dengan nilai Water Contact Angle dari 48,50 ke 46,60, Water Uptake dari 8,1% ke 11,7%. PIM juga bersifat fleksibel dengan nilai Tensile Strength dari 10,7 ke 5,6 Mpa dan %Elongation dari 172% ke 117,3%.
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References
DAFTAR PUSTAKA
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processes: its suitability and mechanisms. Petroleum and Coal, 52(2): 69-80.
2. Almeida, M.I.G.S., Cattrall, R. W., dan Kolev, S. D. 2012. Recent trends in extraction and
transport of metal ions using polymer inclusion membranes (PIMs). Journal of Membrane
Science, 415-416: 9–23.
3. Anggraeni, A., Mutalib, A., Primadhini, dan Bahti, H.H. 2015. Ekstraksi gadolinium(III) dan
samarium(III) dengan pelarut n-heksana melalui pembentukan kompleks dengan ligan
asam di- (2-etilheksil) fosfat. Chimica et Natura Acta, 3(2): 80-83.
4. Aziz, M., Arifin N.F.T., dan Lau W.J. 2019. Preparation and characterization of improved
hydrophilic polyethersulfone/reduced graphene oxide membrane. Malaysian Journal of
Analytical Sciences, 23(3): 479-487.
5. Badan Standardisasi Nasional. 2009. Air dan Air Limbah - Bagian 4: Cara Uji besi (Fe)
Secara Spektrofotometri Serapan Atom (SSA)-Nyala. Badan Standardisasi Nasional, 1–9.
6. Bahmid, N, A., Khaswar, S., Maddu, A. 2014. Pengaruh ukuran serat selulosa asetat dan
penambahan dietilen glikol (DEG) terhadap sifat fisik dan mekanik bioplastik. Jurnal
Teknologi Industri Pertanian, 24(3): 226-234.
7. Bahrami, S., Dolatyari, L., Jam, H.S.,Yaftian, M.R. 2022. Membrane extraction of V(V) by
an oleic acid plasticized poly (vinyl chloride)/Aliquat® 336 polymer inclusion membrane.
Journal of Applied Polymer Science, 139:52434.
8. Carner, C.A. Croft, C.F., Kolev, S.D., dan Almeida, M.I.G.S. 2020. Green solvents for the
fabrication of polymer inclusion membranes (PIMs). Separation and Purification
Technology, 239: 1–7.
9. Govindappa, H., Bhat, M.P., Uthappa, U.T., Sriram, G., Altalhi, T., Kumar, S.P., Kurkuri, M.
2022. Fabrication of a novel polymer inclusion membrane from recycled polyvinyl chloride
for the real-time extraction of arsenic (V) from water samples in a continuous process.
Chemical Engineering Research and Design, 182: 145-156.
10. Harefa, N. 2018. Sensitivitas ligan ditizon terhadap absorbsi logam zink dengan teknik
emulsi membran cair. Jurnal EduMatSains, 3(1): 57-68.
11. Harumarani, S., dan Ma'ruf, W. F. 2016. Pengaruh perbedaan konsentrasi gliserol pada
karakteristik edible film komposit semirefined karagenan eucheuma cottoni dan
beeswax. Jurnal Pengolahan dan Bioteknologi Hasil Perikanan, 5(1): 101-105.
12. Hoque, B., Almeida, M.I.G.S., Cattrall, R.W., Gopakumar, T.G., dan Kolev, S.D. 2019.
Effect of cross-linking on the performance of polymer inclusion membranes (PIMs) for the extraction, transport and separation of Zn (II). Journal of Membrane Science, 589: 117256.
13. Izak, P., Hovorka, S., Bartovský, T., Bartovská, L., dan Crespo, J.G. 2007. Swelling of
polymeric membranes in room temperature ionic liquids, Jurnal of Membrane Science,
296(1-2): 131-138.
14. Jha, R., Rao, M. D., Meshram, A., Verma, H. R., dan Singh, K. K. 2020. Potential of polymer
inclusion membrane process for selective recovery of metal values from waste printed
circuit boards: A review. Journal of Cleaner Production, 265: 121621.
15. Jia, P., Hu, L., Shang, Q., Wang, R., Zhang, M., dan Zhou, Y. 2017. Self-plasticization of
PVC materials via chemical modification of mannich base of cardanol butyl ether. ACS
Sustainable Chemistry and Engineering. 5(8): 6665- 6673.
16. Keskin, B., Gökoğlu, B.Z., dan Koyuncu, I. 2021. Polymer inclusion membrane applications
for transport of metal ions: A critical review. Chemosphere, 279: 130604.
17. Kislik, V.S. 2010. Liquid membranes principles and applications in chemical separations
and wastewater treatment. Elsevier.
18. Kiswandono, A. A., Siswanta, D., Aprilita, N. H., Santosa, S. J., dan Hayashita, T. 2013.
Extending the life time of polymer inclusion membrane containing copoly (eugenol-DVB) as
carrier for phenol transport. Indonesian Journal of Chemistry, 13(3): 254-261.
19. Kolev, S.D., Baba, Y., Cattrall, R.W., Tasaki, T., Pereira, N., Perera, J. M., dan Stevens, G.
W. 2009. Solid phase extraction of zinc(II) using a PVC-based polymer inclusion membrane
with di(2-ethylhexyl)phosphoric acid (D2EHPA) as the carrier. Talanta, 78(3): 795-799.
20. Li, C., Jia, Y., Lu, X., and Chen, H. 2023. Transport of Zn (Ⅱ) through matrix enhanced
polymer inclusion membrane containing OHA and D2EHPA. Chemical Engineering
Journal, 452: 139288.
21. Lusiana, R. A., Sangkota, V. D. A., dan Santosa, S. J. 2018. Chitosan succinate/PVA-PEG
membrane: preparation, characterization and permeation ability test on creatinine. Jurnal
Kimia Sains dan Aplikasi, 21(2): 80-4.
22. Maiphetlho, K., Chimuka, L., Tutu, H., and Richards, H. 2021. Technical design and
optimisation of polymer inclusion membranes (PIMs) for sample pre-treatment and passive
sampling: A review. Science of the Total Environment, 799: 149483.
23. Maiphetlho, K., Shumbula, N., Motsoane, N., Chimuka, L., dan Richards, H. 2020.
Evaluation of silver nanocomposite polymer inclusion membranes (PIMs) for trace metal
transports: selectivity and stability studies. Journal of Water Process Engineering, 37:
101527.
24. Masta, N. 2020. Buku Materi Pembelajaran Scanning Electron Microscopy. Jakarta:
Fakultas Keguruan dan Ilmu Pendidikan Universitas Kristen Indonesia.
25. Miguel, E.R.D.S., Aguilar, J. C., dan Gyves, J.D. 2008. Structural effects on metal ion
migration across polymer inclusion membranes: dependence of transport profiles on nature of active plasticizer. Journal of membrane science, 307(1): 105-116.
26. Mone, C.M. 2023. Penggunaan asam oleat sebagai alternatif plasticizer alami dalam
pembuatan dan karakterisasi polymer inclusion membrane (PIM). Skripsi. Kupang:
Universitas Nusa Cendana.
27. Nghiem, L.D., Mornane, P., Potter, I.D., Perera, J.M., Cattrall, R.W., dan Kolev, S.D. 2006.
Extraction and transport of metal ions and small organic compounds using polymer
inclusion membranes (PIMs). Journal of Membrane Science, 281: 7–41.
28. Nitti, F., Selan, O.T.E., Hoque, B., Tambaru, D., dan Junaidi, M.C. 2022. Improving the
performance of polymer inclusion membranes in separation process using alternative base
polymers : A Review. Indonesian journal of chemistry, 22(1): 284-302.
29. Oluwasola, E.I., Ahmad, A.L., Shoparwe, N.F. 2022. Preliminary study on the stability of
self plasticised thin-flat pim for the extraction of 2-(4-isobutylphenyl) propanoic acid
(ibuprofen). Journal of membrane science and research, 8: 553756.
30. Oluwasola, E.I., Ahmad, A.L., Shoparwe, N.F., dan Ismail, S. 2023. Synergistic tetracycline
removal using dual-polymers based PIM doped with graphene oxide. Materials Today:
Proceedings.
31. Rensini, W.A., Kadang, Luther., Lapailaka, T., Naat, J.N., Pingak, R.K., Kapitan, O.B., dan
Nitti, F. 2024. Uji Stabilitas Polymer Inclusion Membrane dari Polimer Pendukung PVC,
Ekstraktan D2EHPA, dan Plasticizer Asam Oleat pada Kondisi Asam. Jurnal βeta Kimia,
1(4): 1-18.
32. Resina, M., Macanás, J., Gyves, J.D., Munoz, M. 2006. Zn (II), Cd (II) and Cu (II) separation
through organic–inorganic hybrid membranes containing di-(2-ethylhexyl) phosphoric acid
or di-(2-ethylhexyl) dithiophosphoric acid as a carrier. Journal of membrane science, 268:
57-64.
33. Roberts, P.H. dan Thomas, K. V. 2006. The occurrence of selected pharmaceuticals in
wastewater effluent and surface waters of the lower Tyne catchment. Science of the total
environment, 356(1-3): 143-153.
34. Rozitawati, S. P., dan Noerochim, L. 2014. Karakterisasi Membran Polimer dengan
Adsorben Inorganik Lithium Mangan Spinel untuk Ekstraksi Lithium dari Lumpur
Sidoarjo. Jurnal Teknik Pomits, (2), F221-F225.
35. Rusdiarso, B. 2007. Studi ekstraksi pelarut emas (III) dalam larutan konsentrat tembaga
PT freeport dengan 8-metylxantin. Berkala MIPA, 17(2): 15-22.
36. Sellami, F., Senhadji, O.K., Marais, S., Couvrat, N., dan Fatyeyeva, K. 2019. Polymer
inclusion membranes based on CTA/PBAT blend containing aliquat 336 as extractant for
removal of Cr(VI): Efficiency, stability and selectivity. Reactive and functional polymers,
139: 120-132.
37. Sellami, F., Senhadji, O. K., Marais, S., dan Fatyeyeva, K. 2022. PVC/EVA-based polymer inclusion membranes with improved stability and Cr(VI) extraction capacity: Water
plasticization effect. Journal of hazardous materials, 436: 129069.
38. Thaiyibah, N., Alimuddin, A., dan Panggabean, A. S. 2016. Pembuatan dan karakterisasi
membran selulosa asetat-pvc dari eceng gondok (eichhornia crassipes) untuk adsorpsi
logam tembaga(II). Jurnal Kimia Mulawarman, 14(1).
39. Wahyuningtyas, M., dan Atmaja, L. 2016. Pembuatan dan karakterisasi film pati kulit ari
singkong/kitosan dengan plasticizer asam oleat. Indonesian Journal of Chemical
Science, 5(1): 28-35.
40. Wassi, E.U., Nitti, F., Ola, P.D. 2024. Ekstraksi Zn(II) menggunakan polymer inclusion
membrane (PIM) dari resin polivinil klorida (RPVC) dan di(2-ethylhexyl) phosphoric acid
(D2EHPA). Skripsi. Kupang: Universitas Nusa Cendana.
1. Abedini, R. dan Nezhadmoghadam, A. 2010. Application of membrane in gas separation
processes: its suitability and mechanisms. Petroleum and Coal, 52(2): 69-80.
2. Almeida, M.I.G.S., Cattrall, R. W., dan Kolev, S. D. 2012. Recent trends in extraction and
transport of metal ions using polymer inclusion membranes (PIMs). Journal of Membrane
Science, 415-416: 9–23.
3. Anggraeni, A., Mutalib, A., Primadhini, dan Bahti, H.H. 2015. Ekstraksi gadolinium(III) dan
samarium(III) dengan pelarut n-heksana melalui pembentukan kompleks dengan ligan
asam di- (2-etilheksil) fosfat. Chimica et Natura Acta, 3(2): 80-83.
4. Aziz, M., Arifin N.F.T., dan Lau W.J. 2019. Preparation and characterization of improved
hydrophilic polyethersulfone/reduced graphene oxide membrane. Malaysian Journal of
Analytical Sciences, 23(3): 479-487.
5. Badan Standardisasi Nasional. 2009. Air dan Air Limbah - Bagian 4: Cara Uji besi (Fe)
Secara Spektrofotometri Serapan Atom (SSA)-Nyala. Badan Standardisasi Nasional, 1–9.
6. Bahmid, N, A., Khaswar, S., Maddu, A. 2014. Pengaruh ukuran serat selulosa asetat dan
penambahan dietilen glikol (DEG) terhadap sifat fisik dan mekanik bioplastik. Jurnal
Teknologi Industri Pertanian, 24(3): 226-234.
7. Bahrami, S., Dolatyari, L., Jam, H.S.,Yaftian, M.R. 2022. Membrane extraction of V(V) by
an oleic acid plasticized poly (vinyl chloride)/Aliquat® 336 polymer inclusion membrane.
Journal of Applied Polymer Science, 139:52434.
8. Carner, C.A. Croft, C.F., Kolev, S.D., dan Almeida, M.I.G.S. 2020. Green solvents for the
fabrication of polymer inclusion membranes (PIMs). Separation and Purification
Technology, 239: 1–7.
9. Govindappa, H., Bhat, M.P., Uthappa, U.T., Sriram, G., Altalhi, T., Kumar, S.P., Kurkuri, M.
2022. Fabrication of a novel polymer inclusion membrane from recycled polyvinyl chloride
for the real-time extraction of arsenic (V) from water samples in a continuous process.
Chemical Engineering Research and Design, 182: 145-156.
10. Harefa, N. 2018. Sensitivitas ligan ditizon terhadap absorbsi logam zink dengan teknik
emulsi membran cair. Jurnal EduMatSains, 3(1): 57-68.
11. Harumarani, S., dan Ma'ruf, W. F. 2016. Pengaruh perbedaan konsentrasi gliserol pada
karakteristik edible film komposit semirefined karagenan eucheuma cottoni dan
beeswax. Jurnal Pengolahan dan Bioteknologi Hasil Perikanan, 5(1): 101-105.
12. Hoque, B., Almeida, M.I.G.S., Cattrall, R.W., Gopakumar, T.G., dan Kolev, S.D. 2019.
Effect of cross-linking on the performance of polymer inclusion membranes (PIMs) for the extraction, transport and separation of Zn (II). Journal of Membrane Science, 589: 117256.
13. Izak, P., Hovorka, S., Bartovský, T., Bartovská, L., dan Crespo, J.G. 2007. Swelling of
polymeric membranes in room temperature ionic liquids, Jurnal of Membrane Science,
296(1-2): 131-138.
14. Jha, R., Rao, M. D., Meshram, A., Verma, H. R., dan Singh, K. K. 2020. Potential of polymer
inclusion membrane process for selective recovery of metal values from waste printed
circuit boards: A review. Journal of Cleaner Production, 265: 121621.
15. Jia, P., Hu, L., Shang, Q., Wang, R., Zhang, M., dan Zhou, Y. 2017. Self-plasticization of
PVC materials via chemical modification of mannich base of cardanol butyl ether. ACS
Sustainable Chemistry and Engineering. 5(8): 6665- 6673.
16. Keskin, B., Gökoğlu, B.Z., dan Koyuncu, I. 2021. Polymer inclusion membrane applications
for transport of metal ions: A critical review. Chemosphere, 279: 130604.
17. Kislik, V.S. 2010. Liquid membranes principles and applications in chemical separations
and wastewater treatment. Elsevier.
18. Kiswandono, A. A., Siswanta, D., Aprilita, N. H., Santosa, S. J., dan Hayashita, T. 2013.
Extending the life time of polymer inclusion membrane containing copoly (eugenol-DVB) as
carrier for phenol transport. Indonesian Journal of Chemistry, 13(3): 254-261.
19. Kolev, S.D., Baba, Y., Cattrall, R.W., Tasaki, T., Pereira, N., Perera, J. M., dan Stevens, G.
W. 2009. Solid phase extraction of zinc(II) using a PVC-based polymer inclusion membrane
with di(2-ethylhexyl)phosphoric acid (D2EHPA) as the carrier. Talanta, 78(3): 795-799.
20. Li, C., Jia, Y., Lu, X., and Chen, H. 2023. Transport of Zn (Ⅱ) through matrix enhanced
polymer inclusion membrane containing OHA and D2EHPA. Chemical Engineering
Journal, 452: 139288.
21. Lusiana, R. A., Sangkota, V. D. A., dan Santosa, S. J. 2018. Chitosan succinate/PVA-PEG
membrane: preparation, characterization and permeation ability test on creatinine. Jurnal
Kimia Sains dan Aplikasi, 21(2): 80-4.
22. Maiphetlho, K., Chimuka, L., Tutu, H., and Richards, H. 2021. Technical design and
optimisation of polymer inclusion membranes (PIMs) for sample pre-treatment and passive
sampling: A review. Science of the Total Environment, 799: 149483.
23. Maiphetlho, K., Shumbula, N., Motsoane, N., Chimuka, L., dan Richards, H. 2020.
Evaluation of silver nanocomposite polymer inclusion membranes (PIMs) for trace metal
transports: selectivity and stability studies. Journal of Water Process Engineering, 37:
101527.
24. Masta, N. 2020. Buku Materi Pembelajaran Scanning Electron Microscopy. Jakarta:
Fakultas Keguruan dan Ilmu Pendidikan Universitas Kristen Indonesia.
25. Miguel, E.R.D.S., Aguilar, J. C., dan Gyves, J.D. 2008. Structural effects on metal ion
migration across polymer inclusion membranes: dependence of transport profiles on nature of active plasticizer. Journal of membrane science, 307(1): 105-116.
26. Mone, C.M. 2023. Penggunaan asam oleat sebagai alternatif plasticizer alami dalam
pembuatan dan karakterisasi polymer inclusion membrane (PIM). Skripsi. Kupang:
Universitas Nusa Cendana.
27. Nghiem, L.D., Mornane, P., Potter, I.D., Perera, J.M., Cattrall, R.W., dan Kolev, S.D. 2006.
Extraction and transport of metal ions and small organic compounds using polymer
inclusion membranes (PIMs). Journal of Membrane Science, 281: 7–41.
28. Nitti, F., Selan, O.T.E., Hoque, B., Tambaru, D., dan Junaidi, M.C. 2022. Improving the
performance of polymer inclusion membranes in separation process using alternative base
polymers : A Review. Indonesian journal of chemistry, 22(1): 284-302.
29. Oluwasola, E.I., Ahmad, A.L., Shoparwe, N.F. 2022. Preliminary study on the stability of
self plasticised thin-flat pim for the extraction of 2-(4-isobutylphenyl) propanoic acid
(ibuprofen). Journal of membrane science and research, 8: 553756.
30. Oluwasola, E.I., Ahmad, A.L., Shoparwe, N.F., dan Ismail, S. 2023. Synergistic tetracycline
removal using dual-polymers based PIM doped with graphene oxide. Materials Today:
Proceedings.
31. Rensini, W.A., Kadang, Luther., Lapailaka, T., Naat, J.N., Pingak, R.K., Kapitan, O.B., dan
Nitti, F. 2024. Uji Stabilitas Polymer Inclusion Membrane dari Polimer Pendukung PVC,
Ekstraktan D2EHPA, dan Plasticizer Asam Oleat pada Kondisi Asam. Jurnal βeta Kimia,
1(4): 1-18.
32. Resina, M., Macanás, J., Gyves, J.D., Munoz, M. 2006. Zn (II), Cd (II) and Cu (II) separation
through organic–inorganic hybrid membranes containing di-(2-ethylhexyl) phosphoric acid
or di-(2-ethylhexyl) dithiophosphoric acid as a carrier. Journal of membrane science, 268:
57-64.
33. Roberts, P.H. dan Thomas, K. V. 2006. The occurrence of selected pharmaceuticals in
wastewater effluent and surface waters of the lower Tyne catchment. Science of the total
environment, 356(1-3): 143-153.
34. Rozitawati, S. P., dan Noerochim, L. 2014. Karakterisasi Membran Polimer dengan
Adsorben Inorganik Lithium Mangan Spinel untuk Ekstraksi Lithium dari Lumpur
Sidoarjo. Jurnal Teknik Pomits, (2), F221-F225.
35. Rusdiarso, B. 2007. Studi ekstraksi pelarut emas (III) dalam larutan konsentrat tembaga
PT freeport dengan 8-metylxantin. Berkala MIPA, 17(2): 15-22.
36. Sellami, F., Senhadji, O.K., Marais, S., Couvrat, N., dan Fatyeyeva, K. 2019. Polymer
inclusion membranes based on CTA/PBAT blend containing aliquat 336 as extractant for
removal of Cr(VI): Efficiency, stability and selectivity. Reactive and functional polymers,
139: 120-132.
37. Sellami, F., Senhadji, O. K., Marais, S., dan Fatyeyeva, K. 2022. PVC/EVA-based polymer inclusion membranes with improved stability and Cr(VI) extraction capacity: Water
plasticization effect. Journal of hazardous materials, 436: 129069.
38. Thaiyibah, N., Alimuddin, A., dan Panggabean, A. S. 2016. Pembuatan dan karakterisasi
membran selulosa asetat-pvc dari eceng gondok (eichhornia crassipes) untuk adsorpsi
logam tembaga(II). Jurnal Kimia Mulawarman, 14(1).
39. Wahyuningtyas, M., dan Atmaja, L. 2016. Pembuatan dan karakterisasi film pati kulit ari
singkong/kitosan dengan plasticizer asam oleat. Indonesian Journal of Chemical
Science, 5(1): 28-35.
40. Wassi, E.U., Nitti, F., Ola, P.D. 2024. Ekstraksi Zn(II) menggunakan polymer inclusion
membrane (PIM) dari resin polivinil klorida (RPVC) dan di(2-ethylhexyl) phosphoric acid
(D2EHPA). Skripsi. Kupang: Universitas Nusa Cendana.
Published
2025-05-08
How to Cite
Nitti, F., ., S., & Kedang, Y. (2025). PERBANDINGAN KARAKTERISTIK PIM BERBASIS POLIVINIL KLORIDA, DI-(2- ETHYLHEXYL) PHOSPHORIC ACID DAN ASAM OLEAT SEBELUM DAN SESUDAH EKSTRAKSI Zn(II) DALAM SUASANA ASAM. Chemistry Notes, 6(1), 24-38. https://doi.org/10.35508/cn.v6i1.20443
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